The PCB Analyser for Transformer Oil is a dedicated analytical solution designed for the detection and quantification of Polychlorinated Biphenyls (PCBs) in insulating oils. PCBs are persistent environmental pollutants that were historically used in transformer oils due to their excellent dielectric properties. Because of their toxicity and long-term environmental impact, strict monitoring and regulatory control of PCB contamination are essential.
The system is designed in accordance with ASTM D4059 and utilizes Gas Chromatography with Electron Capture Detection (GC-ECD) to provide highly sensitive and selective analysis of PCB compounds. The Electron Capture Detector offers exceptional performance for chlorinated compounds, enabling reliable trace-level detection with minimal interference from the transformer oil matrix.
Sample preparation typically involves dilution of the oil sample with solvents such as hexane or iso-octane, followed by an optional clean-up procedure using silica gel or Florisil columns to remove interfering substances. After preparation, the sample is introduced into the GC-ECD system, where PCB compounds are separated on a dedicated Restek Rtx-PCB column and quantified by comparison with certified Aroclor standards under identical analytical conditions.
The analyzer is based on the robust Thermo Scientific GC 1600 platform, combined with the powerful Chromeleon® Chromatography Data System (CDS) for automated data acquisition, peak grouping, quantification, and reporting. Optional automation features, including the TriPlus RSH or AS 1610 autosampler and automated sample preparation systems, further enhance productivity and throughput for routine laboratory operations.
With its high sensitivity, excellent repeatability, and compliance with ASTM and environmental regulations, the PCB Analyser provides a reliable and cost-effective solution for transformer oil quality control, environmental monitoring, regulatory compliance testing, and laboratory analysis.
| Category | Specification |
|---|---|
| Application | PCB analysis in transformer and insulating oils |
| Standard Method | ASTM D4059 |
| Analytical Technique | Gas Chromatography with Electron Capture Detection (GC-ECD) |
| GC Platform | Thermo Scientific GC 1600 / 1610 Series |
| Injector | Split / Splitless Injector |
| Detector | Electron Capture Detector (ECD) |
| Separation Column | Restek Rtx-PCB Capillary Column |
| Data System | Chromeleon® CDS |
| Sample Preparation | Dilution with hexane or iso-octane; optional silica gel/Florisil cleanup |
| Quantification Method | Comparison with certified Aroclor standards |
| Optional Autosampler | TriPlus RSH or AS 1610 |
| Optional Features | Automated sample preparation, moisture sensors, pressure sensors, cryo valves |
| Compliance | ASTM D4059, EPA and environmental monitoring regulations |
Transformer Oil Quality Control
Monitor PCB contamination in insulating oils to ensure equipment reliability and environmental safety.
Regulatory Compliance Testing
Perform PCB analysis according to ASTM D4059 and environmental regulations.
Sample Screening & Batch Verification
Rapidly screen transformer oil samples prior to maintenance, recycling, or disposal.
Routine Laboratory Analysis
Support high-throughput PCB testing with automated workflows and reproducible results.
Environmental Monitoring
Assess contamination levels in transformer oils to support environmental protection programs.
Research & Analytical Laboratories
Perform advanced PCB characterization with integrated data processing and reporting tools.
- ASTM D4059 – Standard Test Method for Analysis of PCBs in Insulating Liquids.
